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Micro-Thermal Conductivity Detectors (µTCDs) have been designed, fabricated and tested in a gas chromatography system to show a correlation between detector design and the mean free path of the carrier gas. Our tests show that for a fixed detector design, the maximum possible response is limited by the Knudsen number (the ratio of the mean free path of the gas and chamber critical dimensions). Therefore,...
We have developed a novel, calibration free, micro electromechanical device and method for the measurement of linear flow rate in a micro-gas chromatography (GC) system This design enables the integration of a flow rate measurement with a high sensitivity thermal conductivity detector (TCD) reported at MEMS 2009. Accurate knowledge of the flow rate is of vital importance when quantifying the results...
Design, fabrication and testing of a micro thermal conductivity detector (muTCD) with a detection limit of 260 parts per billion (hexane in helium), no excess dead-volume, low power consumption, fast response time (150 musec) and low sensitivity to flow rate is described herein. Significantly, this muTCD is shown to have a linear response and high sensitivity across a 104-fold concentration range;...
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