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A new oxo-centered heterotrinuclear complex [Cr 2 MnO(PhCOO) 6 Py 3 ][CrO 3 Cl] was synthesized, which exhibited weak antiferromagnetic interaction between three atoms Cr III , Cr III and Mn III . The J values for Cr III --Mn III and Cr III --Cr II ...
Pr4V5Si4O22, a new praseodymium vanadium oxosilicate with chevkinite structure, has been prepared by heating PrOCL/V2O5/NH4Cl in an evacuated silica tube; the source of silicon is the reaction tube. It crystallizes in the monoclinic space group C2/m(No. 12) with cell dimensions a = 13.410(2), b = 5.5998(9), c = 11.027(3) Å, β = 100.57(2)°, V = 814.0(5) Å3, and Z = 2, Dcalc = 5.23 g/cm3. The structure...
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