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0.57(Bi0.8La0.2)FeO3-0.43PbTiO3 (BLF-PT) ceramics were successfully prepared by sol-gel technique combined with solid-state reaction method. X-ray diffraction (XRD) results revealed that single crystallites with rhombohedral phase could be obtained at 600 °C for 2 h, which is 150 °C lower than that required to prepare single phase material with the same composition from solid-state reactions. The...
The processes for the physical vapor deposition (PVD) of Pb(Zr,Ti)O3 (PZT) thin films from two different composite oxide targets has been demonstrated. PZT thin films have been deposited by both PVD or sputter technique and standard sol-gel method. Half micron PZT films were deposited by both methods on identical substrates (Si[(100) 4 inch Cz wafer]/SiO2/Ti-TiO2/Pt) followed by sputter-deposited...
A novel piezoelectric microbalance biosensor based on nano-crystalline PZT/quarts is fabricated. Sol-gel method is utilized to bond the PZT thin films on the quartz substrate as the sensing unit. The microstructure and the surface appearance of PZT thin films on quartz substrate and the influence of cancer cells detecting with the sensing unit using PZT/quartz are studied. The XRD and AFM results...
0.68BiFeO3-0.32PbTiO3 (BFPT) films were prepared on SiO2/Si and Pt/Ti/SiO2/Si substrates by sol-gel method. The XRD patterns of BFPT films show that BFPT films have good crystalline properties, and there are no other peaks of impure phases except for the peaks of BFPT thin film and the substrates. The thickness of BFPT thin films that annealed at 600? for 10 min was about 860 nm when deposited 8 layers...
BiFeO3 -PbTiO3 (BFO-PT) films were synthesized by sol-gel method with the annealing temperatures to be 550degC, 600degC, and 650degC, respectively. The structure and morphology of the films were characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM). The dielectric constant and loss factor are measured. The leakage current density is also performed to check the conductivity...
In this research, by adding methyl alcohol/water solution with certain concentration into sol to hydrolysis directly and sintering the fresh gel directly, lead titanate ceramics doped with calcium are prepared by using calcium acetate as doper to prohibit the disadvantages contained in conventional sol-gel method, such as low hydrolytic rate, high sintering temperature, long preparation period. The...
Nd3+ doped PbZr0.52Ti0.48O3 (PNZT) nanopowders were prepared by sol-gel methods in ethylene glycol system. Neodymium nitrate was used as Nd3+ source. The reaction mechanisms of nanopowder preparing process from the sol were discussed through using FTIR, XRD, TG-DTA, and it was proved that the heating temperature of PNZT was 50degC-100degC higher than PZT. PNZT lattice structure was characterized...
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