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The electrochemical quartz crystal microbalance (EQCM) technique has been employed extensively to elucidate the detailed mechanism of the electrochemical reactions which accompany mass changes. An electrode material other than gold, which is widely used in EQCM, is sometimes necessary as a polarizing electrode to study electrochemical processes, for example, Hg for the reduction of organic substances...
A highly ordered single crystal carbon material, highly oriented pyrolytic graphite (HOPG) has been successfully employed as a working electrode in an electrochemical quartz crystal microbalance study. RTV silicone rubber is selected to adhere the HOPG film onto the quartz crystal surface. Such modified quartz crystal can oscillate with stable frequency. The electrode modified in this way has good...
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