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The reaction of (EtO)3SiCl with 1,3‐diphenylpropane‐1,3‐dione in dichloromethane yields an ionic hexacoordinate compound featuring three chelating 1,3‐diphenylpropane‐1,3‐dionato ligands as proven by its X‐ray structure and multinuclear NMR studies in a fast domino reaction. With a proper selection of the solvent (toluene) and the reaction time, the intermediates of the reaction sequence can be selectively...
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