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We report superoxide‐bridged dicobalt(III) complex 1 supported by 13‐membered amide‐based macrocyclic ligand H2LH. Complex 1 displays a sharp radical‐type EPR spectrum (g = 2.031) and a short O–O distance (1.303 Å). Complex 1 can be synthesized by the reaction of in situ generated [Co2+(LH)] species with O2 or KO2 as well as by the reaction of (Et4N)[Co3+(LH)(Cl)2] (2) with KO2. In contrast, analogous...
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