In this paper, a new experimental method of phase interface motion control with time dependent boundary cooling is presented for ice–water solidification problems. A numerical method for inverse heat transfer problems was developed to predict the transient boundary conditions, which produce a prescribed phase interface motion. In the experimental study, the predicted boundary temperatures from the numerical simulation were used to control the ice–water interface movement for various specified interface motions. Two cases of different phase interface velocities were considered. Water supercooling was observed during each experiment. A time delay in the thermal control was calculated based on an analytical solution. Close agreement between measured data and specified interface motion was achieved for the ice–water solidification problems.