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The underpotential deposition of lead was studied on spherical and faceted gold nanoparticles. On 21.7nm spherical nanoparticles, a single stripping peak from Au(111) face was observed at −0.2V, whereas on 82nm faceted gold nanoparticles the peak split in to two at −0.2V and −0.18V vs Ag/AgCl (3M KCl). The roughening of the Au(111) terraces by electrochemical treatment leads to the suppression of...
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