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The electroreduction of nitrobenzene has been studied on Au single crystals of (111), (110), (100), and (210) orientations and on Au polycrystals in dilute aqueous perchlorate solution using cyclic voltammetry. The voltammograms were found to be dependent sensitively on the surface orientation. Notably, the reduction on (110), (210), and (poly) electrodes can lead to a stably adsorbed redox intermediate,...
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