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Novel electrocatalysts for methanol oxidation were prepared from two Pt-Ni multinuclear complexes, [Pt2{Ni(NH2CH2CH2S)2}4]Cl4 and [Pt(bpy){Ni(NH2CH2CH2S)2(bpy)}](NO3)2 (bpy=2,2′-bipyridine). They were adsorbed on a Au(111) surface by immersing the Au(111) electrode in solutions containing these complexes. The modified Au(111) electrodes were then subjected to potential cycling or heat-treatment at...
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