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Developing a facile strategy for constructing oriented mixed matrix membranes (MMMs) with uniformly dispersed and high‐loading metal–organic frameworks (MOFs) is a crucial scientific challenge in probing the enhanced capability and potential applications of MOF‐polymer MMMs. Herein, a novel synchronous synthetic method for constructing oriented CuBDC/poly(m‐phenylenediamine) (CuBDC/PmPD) MMM with...