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The preparation of hybrid materials, namely poly(p‐anisidine)@Clay (poly(pAnis)@Clay) and poly(p‐anisidine)@cetyltrimethylammoniumbromide‐Clay (poly(pAnis)@CTAB‐Clay), prepared by oxidative polymerization process is presented. The formation of nanomaterials has been confirmed by XRF, XPS, FT‐IR, and UV–Vis spectroscopy. Interestingly, the study of the optical band gap energy (Eg) evince lowest value...