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Anginex is a 33‐residue peptide that has been previously demonstrated to possess antiangiogenic properties. To provide a tool to evaluate the regional biodistribution and pharmacokinetics of anginex, and possibly to provide a useful angiogenesis‐targeted radiotracer, we have radiolabeled anginex with fluorine‐18. High specific activity [18F]fluorobenzaldehyde (1.5–4.8 TBq (40–130 Ci)/µmol) was used...