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In this study, manganese ferrite magnetic nanoparticles‐based dispersive solid phase extraction (MF‐MNP‐DSPE) was developed for cadmium determination at trace level by flame atomic absorption spectrometry (FAAS). Manganese ferrite‐based magnetic nanoparticles were synthesized to be used as solid phase extraction sorbent. All the analytical conditions were optimized by univariate optimization approach...