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Bionanocomposites (BNCs) of waxy corn starch, glycerol, and graphene oxide (GO) or graphite oxide (GrO) were prepared by melt mixing. First, the GrO was pre‐exfoliated in a water solution using ultrasound at 1 wt %. Small‐angle X‐ray scattering was used to determinate the interlaminar separation of GrO and transmission electron microscopy, Fourier infrared spectroscopy, and thermogravimetric analysis...