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Photocatalytic reduction of O2 to generate H2O2 shows an excellent environment friendly nature and the controllable H2O2 concentrations and is found the prospect of applications in H2O2‐assisted redox. In this paper, MIL‐68(In) is chosen as a sacrifice precursor to construct a multi‐component photocatalyst of In2O3/In2S3/C by integrated in situ sulfidation and pyrolysis routes. The resulting In2O3...