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The anion‐specific effects of the salting‐in and salting‐out phenomena are extensively observed in hydrogels, whereas the cation specificity of hydrogels is rarely reported. Herein, a multi‐step strategy including borax pre‐gelation, saline soaking, freeze‐drying, and rehydrating is developed to fabricate polyvinyl alcohol gels with cation specificity, exhibiting the specific ordering of effects on...