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The praseodymium and neodymium solubilities in the gallium–tin eutectic melt were measured for the first time in a temperature range of 423–1073 K using a high-temperature sampling technique. The data on the activity and solubility are used to calculate the activity coefficients, the excessive thermodynamic characteristics of α-praseodymium and α-neodymium in the Ga–Sn eutectic melts, and the separation...