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Ag nanoparticles were sputter-deposited on ammonium persulfate ((NH4)2S2O8) powder to obtain (NH4)2S2O8−Ag powder, which was used to synthesize the HCl-doped polyaniline−Ag (HCl−PANI−Ag) composite via a polymerization procedure. The Ag nanoparticles were dispersed in the HCl−PANI matrix, and their sizes mainly ranged from 3 to 6 nm. The Ag nanoparticles did not affect the structure of emeraldine salt...