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The goal of this study was to investigate the structure and optical properties of the prepared PVC/NiO nanocomposites. The samples were characterized via XRD, TEM, SEM, and UV–Vis spectrophotometer experimental measurements. The partial crystal structure of PVC/NiO nanocomposites and cubic structure of NiO nanoparticles were explored by X-ray diffraction. SEM exhibited the good distribution of the...