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It is shown by x-ray diffraction, energy-dispersive x-ray spectrometry, and electron probe microanalysis that, at 800°C, the Ni–P system contains four phosphides in the composition range 25–33 at % P: Ni3P, Ni5P2 , Ni12P5 , and Ni2P. The structure of Ni5P2 is determined by single-crystal x-ray diffraction: sp. gr. P3¯c1, new structure type, a = 0.6613(3) nm, c = 1.2311(6) nm, 347 independent hklreflections...