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Experiments to investigate changes in the sorption behaviour of palladium when aged as β-palladium tritide for a 5.6 year period have been undertaken. The palladium was found to retain a significant quantity of the 3He generated by the decay of tritium (3He/Pd = 0.15) which modified the sorption behaviour. The observations corroborate previous reports of a shift in the α-phase boundary to higher compositions,...