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[ 11 C]TCH346, a compound acting on the glycolytic enzyme, glycerol-aldehyde-3-phosphate dehydrogenase, was produced under optimised conditions by methylation of the desmethyl compound with no-carrier added (n.c.a.) [ 11 C]methyl triflate. An i.v. injectable solution of n.c.a. [ 11 C]TCH346 containing 4040±1550MBq (n=6) containing a molar activity between 40 and 5700GBq/μmol...