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Incorporation of high-loading redox-active materials with small amounts of graphene is a general protocol to achieve high-performance catalysts. Herein, hierarchical MoS2-reduced graphene oxide nanosheet (denoted as MoS2–rGO nanosheets) hybrids with a loading of MoS2 as high as 94wt% are synthesized. The obtained hierarchical MoS2–rGO nanosheets simultaneously integrate the structural and compositional...