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The separation of sugars and sugar alcohols with a strong cation-exchange poly(styrene-co-divinylbenzene) (PS-DVB) resin in the Na + form using subcritical (superheated) water as an eluent was studied in order to elucidate the potential of the technology in the recovery of carbohydrates from hemicelluloses hydrolysates. The separations were carried out on a column having inner diameter 2.2cm...