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In this paper the kinetics of the reaction of [IrCl 5 (H 2 O)] 2- with CH 3 CN has been studied. The reaction product was isolated and identified as K 2 [IrCl 5 (CH 3 CN)] 2H 2 O. The experimental rate constants show no constant order with respect to the acetonitrile concentration. A preferential solvation of [IrCl 5 ...
Rhodium exists in LiCl-KCl melts at 400-450°C as the RhCl 3-6 species. Spectroscopic data show that an increase of the temperature up to 600°C leads to a reaction of this species with the melt and to the formation of the stable Rh(II) chlorocomplex. This reaction, which has not been reported previously, is reversible since on cooling to lower temperatures, 400-450°C, reoxidation...
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