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We report the synthesis and characterization of ZnO nanoparticles prepared via pulse combustion-spray pyrolysis (PC-SP) at a high rate. Instead of using an ultrasonic nebulizer as the atomizer during PC-SP synthesis, a two-fluid nozzle was used to enhance the production rate. A high production rate was achieved by the use of a two-fluid nozzle, which efficiently generated droplets in large quantities,...