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Thermal decomposition of the polydimethylsiloxane-(azobiscyano-pentanoyl ester)s (PDMS-ACP) in the presence of methyl methacrylate (MMA) monomer yielded poly(dimethylsiloxane)-poly(methyl methacrylate) block copolymers (PDMS-b-PMMA). Phosphorus functionalized poly(methyl methacrylate) (DEVP-PMMA) was prepared by copolymerization of MMA with diethyl vinyl phosphonate (DEVP) with PDMS-ACP initiator...
The thermo-oxidative degradation of phosphorus-containing polyurethane (PU) incorporating phenylbis(hydroxyethyl)phosphonate was studied by using thermogravimetric analysis (TGA) and differential thermal analysis (DTA) in oxidizing (air) atmospheres. From the resulting data apparent activation energies (E a ) were obtained following the methods of Flynn, Broido and Ozawa. The activation...
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