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An original way to manage both stereochemistry and conformational constraints in ligand candidates for bioassays is presented with reference to a group of model N,N′-tetrasubstituted o-phthalamides and thioamides. The study shows that a scale of thermal flexibility in solution can be envisaged, the divisions of which are represented by compounds sharing quite similar geometrical features. NMR spectroscopy...
Some tetracyclic compounds containing the pyridodiazepine system condensed with the pyridofuro, pyridothieno and indolo groups were synthesized. In the case of indole derivatives the outcome of the reaction is highly dependent by the nature of the substituents.
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