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Readily available l-menthyl phthalate has been shown to be an effective derivatizing agent for determination of the enantiomeric purity of alkyl- and aryl-substituted 1,1,1-trifluoromethyl-2-alkanols using HPLC and GC. It has been shown that a previously described protocol for one-step enzymatic kinetic resolution results in the formation of the desired 1,1,1-trifluoromethyl-2-alkanols with 96–98%...
An enhancement of palladium-catalyzed Suzuki cross-coupling reactions between substrates possessing long-chain alkyl or oxyalkyl substituents in two-phase media, in the presence of sodium dodecylsulfate, is shown. Quantitative evaluations of the influence of SDS on the reaction rates were determined.
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