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Poly(vinyl chloride) (PVC)-based polymer inclusion membranes (PIMs) containing the commercial anionic extractant Aliquat 336 and in some cases also 1-dodecanol as plasticizer were used for the fabrication of PIM surface-confined Au nanoparticles (NPs) by reduction of Au(III), extracted into the membranes as the [AuCl4]− complex. The experimental conditions controlling Au NP size and distribution were...