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In this study, nano-crystalline Ni 0.6−x Cu x Zn 0.4 Fe 2 O 4 ferrite (0.0⩽x⩽0.5) with grain sizes of 16–38nm have been prepared through a novel method using gelatin. The proper calcination temperature for the precursors which corresponding to the ferrites formation is estimated through thermal analysis measurement. X-ray diffraction patterns confirmed...