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Electropolymerization of terthiophene was carried out in various solvents on carbon fiber microelectrodes, platinum and gold electrodes. Acetonitrile was found to be the most suitable solvent for film formation. The effect of sweep rate and supporting electrolyte on the electropolymerization is discussed. The surface morphology of electrografted carbon fiber microelectrodes was investigated by atomic...
Electropolymerization of tetrathiophene was carried out in various solvents on carbon fiber microelectrodes and platinum electrodes. Acetonitrile, dichloroethane and propylene carbonate were investigated as solvent systems for film formation, and solvent effect as well as the effect of other experimental conditions (scan rate, supporting electrolyte) on the electropolymerization has been discussed...
A new way to synthetize conducting polymers has recently been reported and is investigated further in this study. Poly(2,2':5',2'' terthiophene) is electrochemically prepared at an electrified liquid-iquid interface between two immiscible electrolyte solutions (ITIES) and initiated by a heterogeneous electron transfer (HET) between an aqueous couple (Ce(IV)/Ce(III)) and the 2,2':5',2'' terthiophene...
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