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Nanoparticles are frequently used as targeting delivery systems for therapeutic and diagnostic radiopharmaceuticals. Polyethylene oxide–polyacrylic acid (PEO–PAAc) nanogel was prepared via γ‐radiation‐induced polymerization. Variable factors affecting nanoparticles size were investigated. The nanogel was radiolabeled with the imaging radioisotope 99mTc and finally conjugated with folic acid to target...