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Electrochemical properties of mixed titanium‐niobium oxide TiNb2O7 (TNO) synthesized via vacuum annealing as high potential anode material for lithium‐ion batteries were investigated. Crystal structure, size, and morphology are nearly independent of the annealing atmosphere for starting materials but the color of vacuum‐annealed TNO (TNO‐V) is dark blue while white for the air‐annealed one (TNO‐A)...