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Layered double hydroxides (LDHs) have been designed and applied in environmental remediation based on their tunable physical structure and excellent chemical performance. To investigate the adsorption behavior of aqueous phosphate by the LDH‐based composite, zirconium‐modified Mg‐Al‐LDH (Zr‐LDH) was synthesized by the coprecipitation method, and subsequently calcined to obtain a layered double oxide...