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Shear force‐based scanning electrochemical microscopy is applied for pH monitoring during a sealing reaction at the interface between anodized 7175 aluminium alloy and a solution containing Cr(III) and Zr(IV) species. pH measurement is carried out with the electrode positioned near enough to the surface to be in the diffusion zone of the liquid/solid interface, in the reach of the surface‐generated...
The anodized layer growth in H2SO4 2molL−1 on three different aluminium alloys (1050, 7175, 2618) is investigated by in-situ electrochemical methods and ex-situ characterization techniques.SEM observations of the anodic films indicate that they contain defects related to the size and the composition of the intermetallic phases precipitated within the aluminium matrix. The electrochemical resistances...
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