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The high‐efficient and visible‐light active monoclinic BiVO4 thin films with preferentially oriented (020) facets are successfully deposited by nebulizer spray pyrolysis technique. The role of substrate temperature over crystal growth facets and other physical properties of BiVO4 films are analyzed using XRD, HRTEM, UV spectrometer, and Raman analysis. The BiVO4 thin film deposited at 350 °C possesses...