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Combining the molecular wire effect with a biphasic sensing approach (analyte in water, sensor‐dye in 2‐methyltetrahydrofuran) and a microfluidic flow setup leads to the construction of a mercury‐sensitive module. We so instantaneously detect Hg2+ ions in water at a 500 μM concentration. The sensor, conjugated non‐water soluble polymer 1 (XFPF), merely supports dibutylaniline substituents as binding...