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The modular one‐pot synthesis of a large family of bi‐ and tridentate 2,5‐dimethyl‐ and 2,5‐diphenyl‐substituted phospholanes employs air‐stable chiral phospholanium chloride salts and primary amines or NH4Cl as starting materials. These were transformed into the C2‐symmetric dimethyl‐ and diphenylphospholane ligands, which reacted with [Rh(cod)2]BF4 (cod=1,5‐cyclooctadiene) to yield the rhodium complexes...
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