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The sulfonation of solid acrylonitrile‐butadiene‐styrene, a feedstock that is often used in the 3D printing process of fused filament fabrication, and its application in characterizing liquid‐solid mass transfer is reported. The ion‐exchange capacity was assessed experimentally, and intraparticle diffusion coupled with extraparticle liquid‐solid mass transfer was simulated. Tubular reactors and spherical...