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A fast and efficient microwave (MW)‐assisted solid‐phase peptide synthesis protocol using the 2‐chlorotrityl chloride resin and the Fmoc/tBu methodology, has been developed. The established protocol combines the advantages of MW irradiation and the acid labile 2‐chlorotrityl chloride resin. The effect of temperature during the MW irradiation, the degree of resin substitution during the coupling of...