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The preparation of two different types of PtNi overlayer supported on Pt{111} together with their characterisation by cyclic voltammetry (CV), scanning tunnelling microscopy (STM) and X-ray photoelectron spectroscopy (XPS) is reported. The first PtNi surface was created by resistively heating to approximately 1100K a 10–2M droplet of aqueous nickel (II) chloride solution attached to a Pt{111} Clavilier...
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