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Calcium sulfate is an important construction material. More than 1600 million square meters of interior surfaces are covered with plasterboards in Europe each year. Plasterboard is manufactured by transforming mined or recycled gypsum (CaSO4× 2 H2O) to bassanite (CaSO4× ½H2O) in a time‐ and energy‐consuming heating process. A fast and sustainable way to produce bassanite by solvent‐assisted milling,...