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This paper reports on the operando study of degradation mechanisms in carbon-based electrochemical capacitors with Li2SO4 and LiNO3 electrolytes. Several electrochemical techniques, coupled with mass and Raman spectrometry have been implemented to recognize and describe the processes occurring at the carbon electrode/aqueous electrolyte interface. It has been shown that for the systems operating with...
The near ambient pressure photoemission (NAPP) technique equipped with a liquid jet (LJ) is used for the first time to explore the electronic structure of the most commonly employed carbonate based Li-ion battery electrolytes. Experiments were performed at the SIM beamline of the Swiss Light Source (SLS) with the purpose of monitoring the Li-ion (Li+, Li 1s) solvation of 1M LiClO4 in 1:1 EC:DMC, both...
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