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The main purpose of this work was the synthesis of composite materials by deposition of nickel oxide on 3 mol% yttria-stabilized zirconia (3 mol% Y2O3–97 mol% ZrO2–YSZ) and Sr0.96Y0.04TiO3 (4 mol% Y-doped strontium titanate—SYTO) supports. Yttria-stabilized zirconia and yttrium-doped strontium titanate were obtained by modified citrate method. The deposition of nickel oxide was performed by impregnation...