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This review shows that infra-red spectroscopy is used very much today to unravel the nature of the solid state and the forces operating in crystals. It is clear that the advent of the automatic recording laser Raman spectrometer has enhanced the usefulness of the infra-red spectrometer for solid-state studies. There is still scope for much work, e.g. in the study of phase changes, and especially in...
The crystal structure of a copper antimonite (CuSb2O4) was determined from X-ray powder diffraction data. The structure was solved by simulated annealing in direct space using the Rietveld method. The compound crystallizes in tetragonal symmetry and space group P42bc (106); unit cell parameters a = b = 8.76033(5) Å, c = 5.79786(4) Å, Z = 4, V = 444.947(5) Å3 and density (calc.) = 5.539 g cm−3...
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