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Thiosalicylatodiorganotin, [R2Sn(O2CC6H4S)]n, (R=Me (1), n-Bu (2), Ph (3), 3-Cl–PhCH2 (4)), are prepared from thiosalicylic acid and diorganotin chlorides. All the compounds, 1–4, are characterized by elemental analysis as well as IR and 1H-NMR spectroscopy. X-ray crystallographic analysis of the 2 and 4 shows that the structures are polymeric with neighboring diorganotin centers being linked by...