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The long-term stability of sulfonic acid-containing polyimides has been investigated. The hydrolytic degradation of homopolyimide and the block copolyimide comprising 27 mol% of 2,2′-bis(trifluoromethyl)benzidine and 9 mol% ofm-phenylenediamine (BTFMB27mP10[7/(3+1)]), was quantified through viscosity measurements and FT-IR spectroscopic analyses. The viscosity decrease with respect to time and the...
Several copolyimides have been synthesized with different combinations of comonomers in order to study the relationship between conductivity and water insolubility.m-Phenylenediamine (m-PDA), an angled comonomer, was introduced into the polymer backbone to increase water absorption, and resulted in higher proton conductivity. 2,2-bis(trifluoromethyl)benzidine (TFMB) was used as the comonomer to promote...
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