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The phase structure of the rapidly quenched solid helium samples is studied by the NMR technique in dilute 3He-4He mixtures at 1.35–1.8 K. The pulse NMR method is used to measure the spin-lattice and spin-spin relaxation times for all coexisting phases. An additional spin-lattice relaxation process is found just before vitrification of the liquid inclusions in hcp matrix. The relaxation rate of the...